Please use this identifier to cite or link to this item: http://hdl.handle.net/10397/115283
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Title: Enhancing geometric integrity and surface hardness of SLM-printed Ti-6Al-4V components with support structures and laser nitriding
Authors: Xie, W 
Kirk, C
Rejee, A
Man, H 
Chan, CW
Issue Date: 30-Oct-2024
Source: Surface and coatings technology, 30 Oct. 2024, v. 494, pt. 1, 131378
Abstract: This study investigated the effect of support structure and post-processing surface nitriding on high aspect ratio Ti-6Al-4V components fabricated using Selective Laser Melting (SLM). It examined changes in geometric integrity, porosity, and mechanical properties. Samples were printed without support structures (S1) and with support structures (S2). After SLM printing, both samples underwent open-air laser nitriding at duty cycles (DC) ranging from 50 % to 100 %, aiming to create crack-free nitride layers to increase surface hardness. The results indicated that support structures effectively mitigate thermal-induced deformation, with S2 exhibiting minimal warping and closer adherence to design specifications than S1. Although S2 showed increased porosity as revealed by X-ray Computed Tomography (XCT), its refined microstructure contributed to increased hardness. Optical Microscope and Scanning Electron Microscope (SEM) analyses demonstrated that laser nitriding at a 50 % duty cycle produced uniform, crack-free titanium nitride (TiN) layers. Vickers hardness tests revealed a significant enhancement in the surface hardness of both laser-nitrided samples, with S2 displaying finer TiN dendrites that further improved its surface hardness. The use of support structures was found to be effective in achieving a more uniform microstructure and enhanced hardness in the nitride layer.
Keywords: Laser nitriding
Selective laser melting (slm)
Support structures
Surface hardness
Brinell hardness
Brinell hardness testing
Fracture mechanics
Rockwell hardness
Selective laser melting
Tin alloys
Titanium alloys
Titanium nitride
Vickers hardness
Vickers hardness testing
Crack free
Duty-cycle
Effect of supports
Laser nitriding
Nitride layers
Support structures
Surface hardness
Ti-6al-4v
Aspect ratio
Publisher: Elsevier
Journal: Surface and coatings technology 
ISSN: 0257-8972
EISSN: 1879-3347
DOI: 10.1016/j.surfcoat.2024.131378
Rights: © 2024 The Authors. Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by- nc-nd/4.0/).
The following publication Xie, W., Kirk, C., Rejee, A., Man, H. C., & Chan, C. W. (2024). Enhancing geometric integrity and surface hardness of SLM-printed Ti-6Al-4V components with support structures and laser nitriding. Surface and Coatings Technology, 494, 131378 is available at https://doi.org/10.1016/j.surfcoat.2024.131378.
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