Please use this identifier to cite or link to this item: http://hdl.handle.net/10397/79661
Title: Crystallization temperature investigation of Cu2ZnSnS4 by using Differential scanning calorimetry (DSC)
Authors: Miao, DG
Xu, JT 
Jiang, SX 
Ning, X
Liu, J
Shang, SM 
Keywords: Cu2ZnSnS4
Crystallization
DSC
Anneal
Thermal dynamic
Issue Date: 2018
Publisher: Pergamon Press
Source: Ceramics international, Mar. 2018, v. 44, no. 4, p. 4256-4261 How to cite?
Journal: Ceramics international 
Abstract: The Cu2ZnSnS4 (CZTS) powder was systematically investigated by energy dispersive X-Ray spectroscopy (EDX), X-ray diffraction (XRD), scanning electron microscopy (SEM) and Ramam spectrometer, and further studied by differential scanning calorimetry (DSC), thermogravimetric analysis (TGA). The Ramam and XRD results showed that the sample is a structure of Kesterite type under a condition of Cu-rich and Zn-poor with few impurity phases. The DSC results show that incubation time, peak time and end time of crystallization are all reduced with the increasing temperature; and the temperature of 550 degrees C will be more suitable for annealing treatment of CZTS. A CZTS film is also fabricated and annealed at 550 degrees C to confirm the result of the research. The systematic investigation of CZTS by using differential scanning calorimetry provided a fundamentally dynamic reference for the temperature selection of anneal during the fabrication of CZTS.
URI: http://hdl.handle.net/10397/79661
ISSN: 0272-8842
EISSN: 1873-3956
DOI: 10.1016/j.ceramint.2017.12.006
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